Principles of Chemistry I Laboratory Syllabus for 2011-2012
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Course

CHEM-1111-004 Principles of Chemistry I Laboratory

Prerequisites

CHEM 1311 or concurrent enrollment

Course Description

Includes use of standard laboratory equipment and techniques, both qualitative and quantitative, such as gravimetric analysis, titrations, descriptive chemistry and investigation of gas laws.

Student Resources Student Resources Website

Department Expectations

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Occupational License Disclaimer

Hours

(1 sem hr; 4 lab)

Class Type

On Campus Course

Syllabus Information

Textbooks

\ Laboratory Manual:  Principles of General Chemistry, A. G. Foster, 2003 Revision

Supplies

\ safety goggles, Lab. coat or apron, pencil, pen, scratch paper, calculator

Student Performance

\  Upon successful completion of this course, students will: 

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  1. \ Use basic apparatus and apply experimental methodologies used in the chemistry laboratory.
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  3. \ Demonstrate safe and proper handling of laboratory equipment and chemicals.
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  5. \ Conduct basic laboratory experiments with proper laboratory techniques.
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  7. \ Make careful and accurate experimental observations.
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  9. \ Relate physical observations and measurements to theoretical principles.
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  11. \ Interpret laboratory results and experimental data, and reach logical conclusions.
  12. \
  13. \ Record experimental work completely and accurately in laboratory notebooks and communicate experimental results clearly in written reports.
  14. \
  15. \ Design fundamental experiments involving principles of chemistry.
  16. \
  17. \ Identify appropriate sources of information for conducting laboratory experiments involving principles of chemistry.
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Students Rights and Responsibilities

Student Rights and Responsibilities

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Expected Student Behavior

\ Conduct:  Safety equipment must be worn at all times:  long pants/skirt (covering at least the top half of the calf), apron or lab coat, hair back, safety goggles, and, if necessary, gloves.  No open-toed shoes, shoes with holes in them, shoes that leave the top of the foot exposed, hats of any sort, shorts, food or drink are allowed. Anyone acting in an unsafe manner will be warned once.  If seen without safety equipment or acting improperly a second time, they will be asked to leave the laboratory.  They will be allowed to return in 30 minutes to finish their work, if they can.  If they are asked to leave more than once for any given experiment, they will receive a zero for that experiment’s lab report.  Safety is the MOST important part of lab.  You must attend the safety lecture and pass the safety quiz (with an 80) before you will be allowed to perform experiments for lab.  Any experiments missed by failing to do this will be zeroes and cannot be made up.

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\ Use of previous semester’s work, from whatever source, is considered cheating.  If you have access to such papers, turn them in to the instructor at the beginning of the semester and they will be returned at the end.  If a student is seen to be using any other student’s work, past or present, they will receive a zero grade for that assignment and it cannot be dropped.

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\ Some labs will be done with partners and all will be done in close proximity to other students.  You are encouraged to discuss and/or work with your neighbors; however, working with a student does not give license to simply copy work/data. Please read and abide by the Student Rights and Responsibilities Handbook.

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Grading Criteria

\ Grading:  Lab reports, 65%; Quizzes, 10%; Post-labs, 10% and Exam, 15%.  One low quiz and lab report grade will be dropped.  Attendance in the lab is required, and you must be on time.  Class begins at 9:30.  You must have completed the pre-lab and turn it in at the start of class or you will not be allowed to start an experiment.  Pre-lab assignments will be graded and points will be deducted from the lab report.  A pre-lab lecture will be given at the beginning of each lab experiment. If any of the pre-lab lecture is missed you will not be allowed to start an experiment.  A weekly quiz on the pre-lab will be given at the beginning of lab class—you must be prepared for lab before coming to lab. You must be on time to take the quiz. If you are not present while the quizzes are handed out you will not be able to take the quiz, and receive a zero grade for that quiz.  The post-lab is due following the completion of an experiment at the beginning of the lab period.  Lab reports will either be due at the end of the lab period or at the beginning of the following lab period, depending on the lab.  No late work is accepted.  Exact criteria for grading lab reports will be discussed during the pre-lab.  Dropping the course is the sole responsibility of the student. There are NO make-up labs, no exceptions. Emergencies are the reason for a dropped lab grade.  If you miss lab, you may still turn in a post lab assignment.

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\ You must clean up your area of the lab. It is not the instructor’s or Mr. Crofford’s job to clean up after you.  Failure to leave a clean lab will result in a 10 point deduction on your lab report for that experiment.  If the lab in general is left messy rather than an individual’s area, the whole class may be docked points on their lab report. 

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\ All students are required to clean their laboratory equipment and check out of their locker.  Failure to check out of your locker will result in one letter grade deduction for the course.  Failure to officially withdraw will result in a grade of F.  Grades are based on 90.00+ = A, 80.00-89.99 = B, 70.00-79.99 = C, 60.00-69.99 = D, and 59.99 and lower = F.

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\ All grey areas of the lab reports must be in pen, only.  Whenever writing data, or observations down, it must be written directly into your lab book.  Scratch paper may be used for calculations, if necessary, but if instructed to show all work, you must include it with the lab report.  You CANNOT write data (such as weights, measurements, etc.) on scratch paper then copy it into your lab book.  If you make a mistake while writing in pen, simply cross it out once and write the correct number in close-by.  Do NOT use correction fluid or tape.  If you do make a correction, you MUST come to the instructor and show him the correction so that he can approve it.

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\ Some possible areas to lose points in lab reports are:

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  1. \ significant figures -  2 points                                                          
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  3. \ labels/units -  1 points                                          
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  5. \ calculation errors -  5 points                            
  6. \
  7. \ using white-out -  5 points
  8. \
  9. \ writing in pencil in grey area -  5 points (even if you go back and write over in ink or erase)
  10. \
  11. \ not crossing out once only - 1 to 5 points
  12. \
  13. \ writing data on scratch paper -  5 points
  14. \
  15. \ failure to have cross-out approved -  5 points
  16. \
  17. \ not showing all work when asked -  up to all points
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  19. \ not cleaning up lab -  10 points
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  21. \ error in experimental value -  variable (depends on class average, etc.)
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Attendance

\ Attendance in the lab is required. Make-up labs will occur only with prior permission of the instructor—at least a week’s notice, a valid reason for the absence, and have written approval.  Emergencies are the reason for a dropped lab grade.

Calendar

Outline of Course:  Subject to change

Dates

Experiment

Notes

Aug. 24

Lab. safety & introduction

  • Safety Video
  • Lab Tour
  • Safety Quiz

Aug. 31

#1, Density Measurement

  • Significant Figures
  • Rounding
  • Scientific Notation
  • Math and Significant Figures
  • Measurements and Units
  • Percent Uncertainty

Sept. 7

#2, Nomenclature Drill

  • Nomenclature Rules
  • Name Compounds and Writing Formulas

Sept. 14

#6, Determination of Percent Water in a Hydrate

  • How to find % water given a hydrate formula.
  • Significant Figures
  • Calculating hydrate and anhydrous

Sept. 21

#7, Stoichiometry of Chemical Reactions

  • Write balance equation using correct states
  • Stoichiometric Calculations
  • Significant Figures
  • Percent Yield

         

Sept. 28

 

#4, Precipitation Reactions (and Ionic Equations)

  • What’s a precipitate?
  • Differences in molecular, net ionic, and total ionic equations
  • Solubility rules
  • Ions vs. elements 

Oct. 5

#5, Conductivity in Aqueous Solutions (Please remember to make up solution for lab #8)

  • Strong & Weak Acids/Bases
  • Soluble and Insoluble Salts
  • Writing Balanced Equations
  • Reactions with Acids
  • Strong and Weak Electrolytes

Oct.12

&

Oct. 19

#8, Acid Base Titrations and Determination of Equivalent Weight of Unknown Acid

(2 week lab)

  • Definitions:  end point, indicator, standards, equivalent weight, normality
  • Calculating normality and equivalents
  • Equivalent weight

Oct. 26

#3, Basic and Acidic Oxides

  • What’s an anhydride?
  • States of matter and when to use them
  • Balance Equations
  • Litmus paper

Nov. 2

#9, Molar Volume of Oxygen

  • Ideal Gas Law
  • Percent Error

Nov 9

#10, Equivalent Weight of a Metal

  • Molar Volume of gas at STP

Nov 16

#11, Preparation and Properties of Colloids

  • Definitions:  condensation, dispersion, peptization, emulsion, emulsifying agent, dialysis, Brownian motion, adsorption, protective colloids
  • Filtration

Nov. 30

Laboratory Exam

  • Comprehensive
  • Check out of lab
 

 

Additional Information

\ Efficient Use of Time:  Please be aware that this class is scheduled from 1:00 to 4:20 (Monday).  This is generally more than enough time to finish most labs, but please expect to be in class for the duration of the scheduled time, if not longer.

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\ INFORMATION SHEET/SIGNATURE:  You must fill out and return the provided information sheet.  You must also sign it to signify that you have read and understand the syllabus.  No graded assignments will be returned to you and you will not be shown your overall grades until the signed information sheet is turned in.

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\ ***This syllabus is subject to change.  You will be informed of any changes to the syllabus***    

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Syllabus Created on:

11/30/-1 12:00 AM

Last Edited on:

11/30/-1 12:00 AM